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  1. 学術雑誌掲載済論文
  2. 洋雑誌

Construction of Terminal Conjugated Enynes: Regio- and Stereoselective Syntheses of 3-Alken-1- ynes and 1-Trimethylsilyl-3-alken-1-ynes from Alkenyldialkylboranes and (Trimethylsilyl)ethynyl Bromide

https://kitami-it.repo.nii.ac.jp/records/7175
afe4b489-b8f8-40d3-9254-4a3c0d3d4b2b
名前 / ファイル ライセンス アクション
4605.pdf 4605.pdf (68.2 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2007-05-11
タイトル
言語 en
タイトル Construction of Terminal Conjugated Enynes: Regio- and Stereoselective Syntheses of 3-Alken-1- ynes and 1-Trimethylsilyl-3-alken-1-ynes from Alkenyldialkylboranes and (Trimethylsilyl)ethynyl Bromide
言語
言語 eng
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
アクセス権
アクセス権 open access
アクセス権URI http://purl.org/coar/access_right/c_abf2
著者 Hoshi, Masayuki

× Hoshi, Masayuki

WEKO 36503

en Hoshi, Masayuki

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Shirakawa, Kazuya

× Shirakawa, Kazuya

WEKO 36504

en Shirakawa, Kazuya

Search repository
著者別名
姓名
姓名 星, 雅之
言語 ja
抄録
内容記述タイプ Abstract
内容記述 The cross-coupling reaction of (E)- and (Z)-1-alkenyldialkylboranes with (trimethylsilyl)ethynyl bromide proceeds in the presence of a base and a catalytic amount of Cu(acac)2 under very mild conditions to provide conjugated enynes whose carbon-carbon triple bond is in distal position. The use of 1 M NaOMe as a base exclusively affords both (E)- and (Z)-3-alken-1-ynes with high regio- and stereoselectivity, while the use of LiOH・H2O instead of 1 M NaOMe preferentially gives both (E)- and (Z)-1-trimethylsilyl-3- alken-1-ynes regio- and stereoselectively.
書誌情報 Synlett

巻 2002, 号 7, p. 1101-1104, 発行日 2002-07
DOI
関連識別子
識別子タイプ DOI
関連識別子 http://doi.org/10.1055/s-2002-32604
権利
権利情報 http://www.thieme-connect.de/ejournals/abstract/synthesis/doi/10.1055/s-2002-32604
権利
権利情報 Georg Thieme Verlag, M.Hoshi, K.Shirakawa, Synlett, 2002(7), 2002, 1101-1104. c 2002 Georg Thieme Verlag KG.
フォーマット
内容記述タイプ Other
内容記述 application/pdf
出版者
出版者 Georg Thieme Verlag
著者版フラグ
値 author
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
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