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Preparation of optically pure δ-lactones using diastereomeric resolution with amino acid as resolving agent
https://kitami-it.repo.nii.ac.jp/records/7978
https://kitami-it.repo.nii.ac.jp/records/7978c4afc883-912d-438a-b554-6ca3cd187a31
名前 / ファイル | ライセンス | アクション |
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2015_Preparation of optically pure δ-lactones using diastereomeric resolution with amino acid as resolving agent.pdf (633.8 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2015-09-09 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Preparation of optically pure δ-lactones using diastereomeric resolution with amino acid as resolving agent | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | δ-lactone | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | diastereomeric resolution | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | resolving agent | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | amino acid | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
著者 |
Shimotori, Yasutaka
× Shimotori, Yasutaka× Hoshi, Masayuki× Seki, Syota× Osanai, Takeshi× Okabe, Hayato× Ikeda, Yoshitaka× Miyakoshi, Tetsuo |
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著者別名 | ||||||
姓名 | 霜鳥, 慈岳 | |||||
言語 | ja | |||||
著者別名 | ||||||
姓名 | 星, 雅之 | |||||
言語 | ja | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Synthesis of optically pure δ-lactones by diastereomeric resolution was investigated. Amino acid derivatives, which can be obtained at a relatively low cost, were used as resolving agents. Six optically pure δ-lactones were efficiently synthesized using Cbz-L-alanine without other expensive resolving agents. Both enantiomers of δ-lactone obtained had over 98% enantiomeric excesses. This diastereomeric resolution is very efficient for the preparation of optically pure δ-lactones. | |||||
書誌情報 |
Journal of Oleo Science 巻 64, 号 1, p. 75-90, 発行日 2015 |
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DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | http://doi.org/10.5650/jos.ess14124 | |||||
権利 | ||||||
権利情報 | c 2015 by Japan Oil Chemists' Society | |||||
出版者 | ||||||
出版者 | Japan Oil Chemists' Society (公益社団法人日本油化学会) | |||||
著者版フラグ | ||||||
値 | publisher | |||||
出版タイプ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 |