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Synthesis of bis(alk-3-en-1-ynyl)benzene with either E- or Z-configuration via a one-pot three-component coupling reaction and its optical properties
https://kitami-it.repo.nii.ac.jp/records/7235
https://kitami-it.repo.nii.ac.jp/records/72358be4ce92-5a39-4d64-b672-08df365133df
名前 / ファイル | ライセンス | アクション |
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tl-0609-447.pdf (310.5 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-01-25 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Synthesis of bis(alk-3-en-1-ynyl)benzene with either E- or Z-configuration via a one-pot three-component coupling reaction and its optical properties | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Bis(alk-3-en-1-ynyl)benzene | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Cross-coupling | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Alkenylborane | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | (Trimethylsilyl)ethynyl bromide | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Diiodobenzene | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
著者 |
Hoshi, Masayuki
× Hoshi, Masayuki× Suzuki, Souichi× Saitoh, Shingo× Okimoto, Mitsuhiro× Shirakawa, Kazuya |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A convenient, efficient and stereoselective synthesis of a range of bis(alk-3-en-1-ynyl)benzenes with E- and Z-configuration is described. The protocol involves Cu-mediated cross-coupling reaction of (E)- and (Z)-alk-1-enyldisiamylboranes with (trimethylsilyl)ethynyl bromide and Pd/Cu-catalyzed cross-coupling reaction with diiodobenzene. The sequential cross-coupling reaction proceeds readily under extremely mild conditions in a one-pot manner to afford bis(alk-3-en-1-ynyl)benzenes in good to excellent yields. The optical properties of the products are also described. | |||||
内容記述 | ||||||
内容記述タイプ | Other | |||||
内容記述 | NOTICE: This is the author's version of a work accepted for publication by Elsevier. Changes resulting from the publishing process, including peer review, editing, corrections, structual formatting and other quality control mechanisms , may not be reflected in this document. Changes may have been to this work since it was submitted for publication. | |||||
書誌情報 |
Tetrahedron Letters 巻 41, 号 1, p. 119-124, 発行日 2007-01-01 |
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DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1016/j.tetlet.2006.10.162 | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
出版者 | ||||||
出版者 | Elsevier | |||||
著者版フラグ | ||||||
値 | author | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa |