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  1. 学術雑誌掲載済論文
  2. 洋雑誌

Stereoselective Syntheses of (E)- and (Z)-1-Arylalk-3-en-1-ynes and (E,E)-, (Z,E)-, (E,Z)-, and (Z,Z)-Alka-1,5-dien-3-ynes via a One-pot Multicomponent Coupling Reaction.

https://kitami-it.repo.nii.ac.jp/records/7173
cd04e5b4-b6fa-4a29-9a08-f6718002fc56
名前 / ファイル ライセンス アクション
4613.pdf 4613.pdf (175.5 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2007-05-11
タイトル
言語 en
タイトル Stereoselective Syntheses of (E)- and (Z)-1-Arylalk-3-en-1-ynes and (E,E)-, (Z,E)-, (E,Z)-, and (Z,Z)-Alka-1,5-dien-3-ynes via a One-pot Multicomponent Coupling Reaction.
言語
言語 eng
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
アクセス権
アクセス権 open access
アクセス権URI http://purl.org/coar/access_right/c_abf2
著者 Hoshi, Masayuki

× Hoshi, Masayuki

WEKO 36495

en Hoshi, Masayuki

Search repository
Nakayabu, Hidenori

× Nakayabu, Hidenori

WEKO 36496

en Nakayabu, Hidenori

Search repository
Shirakawa, Kazuya

× Shirakawa, Kazuya

WEKO 36497

en Shirakawa, Kazuya

Search repository
著者別名
姓名
姓名 星, 雅之
言語 ja
抄録
内容記述タイプ Abstract
内容記述 Both 1-arylalk-3-en-1-yne and alka-1,5-dien-3-yne have been synthesized under extremely mild reaction conditions in good to high yields via a sequential Suzuki-type and Sonogashira reaction in a one-pot manner. Thus, the protocol involves Cumediated cross-coupling reaction of (E)- or (Z)- alkenyldisiamylborane with (trimethylsilyl)ethynyl bromide in the presence of 1M-NaOMe and Pd/Cu-catalyzed cross-coupling reaction with aryl or alkenyl iodide in the presence of aqueous n-Bu4NOH. The reaction with aryl iodide is tolerant of a wide variety of functional groups on the aromatic ring and leads to the stereoselective formation of (E)- and (Z)-1-arylalk-3-en-1-ynes. In addition, the reactions with (E)- and (Z)-1-iodoalk-1-enes have accomplished the construction of all possible combinations of geometrical isomers, (E,E)-, (Z,E)-, (E,Z)-, and (Z,Z)- alka-1,5-dien-3-ynes.
書誌情報 Synthesis

巻 2005, 号 12, p. 1991-2007, 発行日 2005-08
DOI
関連識別子
識別子タイプ DOI
関連識別子 http://doi.org/10.1055/s-2005-869955
権利
権利情報 http://www.thieme-connect.de/ejournals/abstract/synthesis/doi/10.1055/s-2005-869955
権利
権利情報 Georg Thieme Verlag, M.Hoshi, H.Nakayabu, K.Shirakawa, Synthesis, 2005(12), 2005, 1991-2007. c 2005 Georg Thieme Verlag KG.
フォーマット
内容記述タイプ Other
内容記述 application/pdf
出版者
出版者 Georg Thieme Verlag
著者版フラグ
値 author
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
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