{"_buckets": {"deposit": "84cdc50d-2d78-42b2-ae59-f034ec6f1bff"}, "_deposit": {"id": "6158", "owners": [], "pid": {"revision_id": 0, "type": "depid", "value": "6158"}, "status": "published"}, "_oai": {"id": "oai:kitami-it.repo.nii.ac.jp:00006158"}, "item_2_alternative_title_18": {"attribute_name": "\u305d\u306e\u4ed6\u306e\u30bf\u30a4\u30c8\u30eb", "attribute_value_mlt": [{"subitem_alternative_title": "Improved method for determination of selenium in anode slime copper electrolytic refiners"}]}, "item_2_biblio_info_6": {"attribute_name": "\u66f8\u8a8c\u60c5\u5831", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "1964-03", "bibliographicIssueDateType": "Issued"}, "bibliographicIssueNumber": "2", "bibliographicPageEnd": "41", "bibliographicPageStart": "35", "bibliographicVolumeNumber": "1", "bibliographic_titles": [{"bibliographic_title": "\u5317\u898b\u5de5\u696d\u5927\u5b66\u7814\u7a76\u5831\u544a"}]}]}, "item_2_description_14": {"attribute_name": "\u30d5\u30a9\u30fc\u30de\u30c3\u30c8", "attribute_value_mlt": [{"subitem_description": "application/pdf", "subitem_description_type": "Other"}]}, "item_2_description_4": {"attribute_name": "\u6284\u9332", "attribute_value_mlt": [{"subitem_description": "Selenium in anode slime\uff0cwas determined by the following treatment. After treating anode slime with KCI0_3-1: 1 (Vol.) HCI\uff0cselenium is quantitatively precipitated in the hydrochloric acid filtrate by addition of FeS0_4-1: 1 HC1 solution and warming on water-bath (\uff1e80\u2103) for 2 hours. The selenium is redissolved with fuming nitric acid and warmed to expel nitrogen oxides.\u3000In the solution\uff0c1 drop of Phenolphthalein solution\uff0c50\uff05 (Wt.) KOH\uff0c0.1 N-HNO_3\uff0c and 0.1 N-KOH are successively and dropwise added until faint pink colur appeares in the  solution (pH nearly equals 8.5)\uff0c then potassium selenite solution is obtained. Add 0.1 N-AgNO_3 to the potassium selenite solution\uff0c and the selenium is quantitatively precipitated as silver selenite. After cooling with ice\uff0c silver selenite is filtered off and washed with  cold water. The excess silver nitrate in the filtrate is potentiometric baek-titrated with 0.1N?KSCN. (Indicatorelectrode is Ag\uff0cusing KNO_3-bridge.)  Selenium was determined with the following accuracy. For metallic selenium\uff0c the error was\u58eb0.0001 (g,) and for selenium in anode slime\uff0cit was less than \u58eb0.0003 (g.).", "subitem_description_type": "Abstract"}]}, "item_2_full_name_3": {"attribute_name": "\u8457\u8005\u5225\u540d", "attribute_value_mlt": [{"nameIdentifiers": [{"nameIdentifier": "31621", "nameIdentifierScheme": "WEKO"}], "names": [{"name": "Toru, FUJITA"}]}, {"nameIdentifiers": [{"nameIdentifier": "31622", "nameIdentifierScheme": "WEKO"}], "names": [{"name": "Yutaka, OHNO"}]}]}, "item_2_publisher_32": {"attribute_name": "\u51fa\u7248\u8005", "attribute_value_mlt": [{"subitem_publisher": "\u5317\u898b\u5de5\u696d\u5927\u5b66"}]}, "item_2_select_15": {"attribute_name": "\u8457\u8005\u7248\u30d5\u30e9\u30b0", "attribute_value_mlt": [{"subitem_select_item": "publisher"}]}, "item_creator": {"attribute_name": "\u8457\u8005", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "\u85e4\u7530, \u5fb9"}], "nameIdentifiers": [{"nameIdentifier": "31619", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "\u5927\u91ce, \u8c4a"}], "nameIdentifiers": [{"nameIdentifier": "31620", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "\u30d5\u30a1\u30a4\u30eb\u60c5\u5831", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2016-11-22"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "1-2-4.pdf", "filesize": [{"value": "2.6 MB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_free", "mimetype": "application/pdf", "size": 2600000.0, "url": {"label": "1-2-4.pdf", "url": "https://kitami-it.repo.nii.ac.jp/record/6158/files/1-2-4.pdf"}, "version_id": "31242117-47e9-4555-aa5f-72cb77cfcc80"}]}, "item_language": {"attribute_name": "\u8a00\u8a9e", "attribute_value_mlt": [{"subitem_language": "jpn"}]}, "item_resource_type": {"attribute_name": "\u8cc7\u6e90\u30bf\u30a4\u30d7", "attribute_value_mlt": [{"resourcetype": "departmental bulletin paper", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "\u967d\u6975\u6ce5\u4e2d\u306e\u30bb\u30ec\u30f3\u5b9a\u91cf\u6cd5\u306e\u6539\u826f", "item_titles": {"attribute_name": "\u30bf\u30a4\u30c8\u30eb", "attribute_value_mlt": [{"subitem_title": "\u967d\u6975\u6ce5\u4e2d\u306e\u30bb\u30ec\u30f3\u5b9a\u91cf\u6cd5\u306e\u6539\u826f"}]}, "item_type_id": "2", "owner": "1", "path": ["7/15/21"], "permalink_uri": "https://kitami-it.repo.nii.ac.jp/records/6158", "pubdate": {"attribute_name": "\u516c\u958b\u65e5", "attribute_value": "2007-04-09"}, "publish_date": "2007-04-09", "publish_status": "0", "recid": "6158", "relation": {}, "relation_version_is_last": true, "title": ["\u967d\u6975\u6ce5\u4e2d\u306e\u30bb\u30ec\u30f3\u5b9a\u91cf\u6cd5\u306e\u6539\u826f"], "weko_shared_id": 3}